HCID 18919896, compound → HCID 18919895, compound

Participants

Reaction Steps

0.165 g (0.0005 mol) of 1-(3-chloro-benzyl)-piperidin-4-yl benzoate was dissolved in 15 ml of ether, filtered, diluted with 0.6 ml of methanol and treated with 5 ml of 1N ethereal HCI. The separated precipitate was filtered off and dried. 0.166 g (90.6%) of 1-(3-chloro-benzyl)-piperidin-4-yl benzoate hydrochloride (1:1) was obtained as white crystals; m.p. 227°-228°.

Provenance & Evidence