Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 12925059 | HCID 12925059 | — |
| Reactant | HCID 18919240 | HCID 18919240 | — |
| Product | HCID 69961015 | HCID 69961015 | 60.8% |
Reaction Steps
To a mixture of 2,3,5-trimethyl-4(3H)-quinazolinone (376 mg) and 4-(4-chlorobenzoyl)benzaldehyde (1.1 g) was added acetic anhydride (0.5 ml) and the mixture was stirred at 140° C. for 2 hours. This reaction mixture was concentrated and the residue was washed with diethyl ether and dried to provide 504 mg of yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05753664 |
|---|
| Source dataset | uspto-grants-1998_05 |
|---|
| ORD ID | ord-e3acc451853247728dcc00cd2826974c |
|---|
| Source note | uspto-grants-1998_05 |
|---|
