Methyl iodide → 131988-14-2

HRID 1291440Notes

Reaction equation

HRID 1291440 reaction equation
[CH3:1][I:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N:15][CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH2:5][CH3:6]>CC(C)=O>[I-:2].[CH2:3]([O:7][C:8]1[C:12]([C:13]2[CH:14]=[N+:15]([CH3:1])[CH:16]=[CH:17][CH:18]=2)=[N:11][S:10][N:9]=1)[CH2:4][CH2:5][CH3:6]

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 15180133HCID 15180133, compound

Product 1

HCID 19075249131988-14-2

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(3-butoxy-1,2,5-thia-diazol-4-yl)pyridine (580 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.60 g (64%).

Workup

  1. customThe title compound precipitated from the solution
  2. filtrationwas collected by filtration
  3. customto yield 0.60 g (64%)

Sources & evidence

ORD record
ord-d5f6aedf54f14ff580be8cbd4af1b136
Source dataset
uspto-grants-1998_05
Patent number
US05753683

Reaction notes

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