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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1291440Generated: October 30, 2026

Methyl iodide → 131988-14-2

https://huagongshe.com/reaction/1291440

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
ReactantHCID 15180133HCID 15180133—
SolventAcetoneHCID 180—
Product131988-14-2HCID 19075249—

Reaction Steps

A mixture of methyl iodide (0.3 ml, 5 mmol) and 3-(3-butoxy-1,2,5-thia-diazol-4-yl)pyridine (580 mg, 2.5 mmol) in acetone (5 ml) was stirred at room temperature for 18 h. The title compound precipitated from the solution and was collected by filtration to yield 0.60 g (64%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05753683
Source datasetuspto-grants-1998_05
ORD IDord-d5f6aedf54f14ff580be8cbd4af1b136
Source noteuspto-grants-1998_05