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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1291473Generated: October 30, 2026

Methyl iodide → 3-(3-(3-Methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodide

https://huagongshe.com/reaction/1291473

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethyl iodideHCID 6328—
Reactant3-(3-(3-Methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)pyridineHCID 19075325—
SolventAcetoneHCID 180—
Product3-(3-(3-Methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)-1-methylpyridinium iodideHCID 19075389—

Reaction Steps

A mixture of methyl iodide (1 ml, 15 mmol) and 3-(3-(3-methyl-2-butenyloxy)-1,2,5-thiadiazol-4-yl)pyridine (3 mmol) in acetone (3 ml) was stirred at room temperature for 18 h. The title compound precipita ted from the solution and was collected by filtration to yield 0.92 g (79%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05753683
Source datasetuspto-grants-1998_05
ORD IDord-68c878d7d18d4afab4c02cb7bb2ffcb0
Source noteuspto-grants-1998_05