Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Aniline | HCID 6115 | — |
| Reactant | [2,2'-Bithiophene]-5-carboxaldehyde | HCID 364428 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53742001 | HCID 53742001 | — |
Reaction Steps
5.0 g of 5-formyl-2,2'-bithiophene was dissolved in 45 ml of benzene. 2.4 ml of aniline was added and refluxed for 24 hours at 85° C. 6.9 g of crude product was obtained after removal of solvent under reduced pressure and the purer product could be obtained by recrystallization with ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05753692 |
|---|
| Source dataset | uspto-grants-1998_05 |
|---|
| ORD ID | ord-7e77fcebfd9642cf9eba90f3293b40fc |
|---|
| Source note | uspto-grants-1998_05 |
|---|
