反应详情

A mixture of 4-(1-decenyl)nitrobenzene (12.2 g), acetic acid (120 ml) and palladium black (0.84 g) was hydrogenated at room temperature and at 3-4 atm for 12 hours. The catalyst was changed and the reaction was continued under the same conditions for 12 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 10.9 g of 4-decylaniline.

1. waitthe reaction was continued under the same conditions for 12 hours
2. filtrationThe catalyst was filtered off
3. concentrationthe filtrate was concentrated under reduced pressure