戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 1291753作成日:2026年10月25日

4-(1-Decenyl)nitrobenzene → 4-Decylaniline

https://huagongshe.com/reaction/1291753

反応式

関与物質

役割名称HCID仕込み量
反応物4-(1-Decenyl)nitrobenzeneHCID 54217323—
触媒PalladiumHCID 23938—
溶媒Acetic AcidHCID 176—
生成物4-DecylanilineHCID 92309100.1%

反応手順

A mixture of 4-(1-decenyl)nitrobenzene (12.2 g), acetic acid (120 ml) and palladium black (0.84 g) was hydrogenated at room temperature and at 3-4 atm for 12 hours. The catalyst was changed and the reaction was continued under the same conditions for 12 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 10.9 g of 4-decylaniline.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05753649
出典データセットuspto-grants-1998_05
ORD IDord-52f5a88888d74dd8b0f6bf94f16d94c9
出典メモuspto-grants-1998_05