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4-(1-Decenyl)nitrobenzene → 4-Decylaniline
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(1-Decenyl)nitrobenzene | HCID 54217323 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Acetic Acid | HCID 176 | — |
| 生成物 | 4-Decylaniline | HCID 92309 | 100.1% |
反応手順
A mixture of 4-(1-decenyl)nitrobenzene (12.2 g), acetic acid (120 ml) and palladium black (0.84 g) was hydrogenated at room temperature and at 3-4 atm for 12 hours. The catalyst was changed and the reaction was continued under the same conditions for 12 hours. The catalyst was filtered off and the filtrate was concentrated under reduced pressure to give 10.9 g of 4-decylaniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05753649 |
| 出典データセット | uspto-grants-1998_05 |
| ORD ID | ord-52f5a88888d74dd8b0f6bf94f16d94c9 |
| 出典メモ | uspto-grants-1998_05 |