HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 18917760, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 4-Morpholinecarbonyl chloride | HCID 84810 | — |
| Reactant | O-benzylglycine toluene-p-sulphonate | HCID 6451311 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18917760 | HCID 18917760 | — |
Reaction Steps
Analogously to Example 7b), 7.69 g (22.8 mmol) of glycine-benzyl ester 4-toluenesulfonate and 2.8 g (19 mmol) of (morpholinocarbonyl)chloride in 118 ml of methylene chloride and 9 ml (53 mmol) of N-ethyldiisopropylamine are reacted for 18 h. The title compound is obtained in pure form after extraction with methylene chloride and digestion with hexane: tRet (I)=11.6 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05753652 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-ed769eddf9c248489c2af233f699a4d1 |
| Source note | uspto-grants-1998_05 |