Pyridine → HCID 53661555, compound

Participants

Reaction Steps

4-(Ethoxyethyl)benzoic acid (1.4 g, 7.2 mmol) was mixed with thionyl chloride (1.3 g, 10.8 mmol), pyridine (0.1 ml) and toluene (4 ml), followed by reacting them at 80° C. for 2 hours, distilling superfluous thionyl chloride and toluene under reduced pressure, to obtain raw 4-(ethoxy-ethyl)benzoyl chloride.

Provenance & Evidence