HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 18914110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 18914102 | HCID 18914102 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18914110 | HCID 18914110 | — |
Reaction Steps
Methyl 2-methyl-4-trifluoromethylnicotinate was reduced using the procedure as given in step 1 of Example 3. 3-Hydroxymethyl-2-methyl-4-trifluoromethylpyridine was obtained as a pale yellow waxy solid(TLC Rf = 0.31 (97:3 CH2Cl2 :MeOH)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756497 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-e8469d2f2471488cb2fd39930724a0ed |
| Source note | uspto-grants-1998_05 |