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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1292049Generated: October 29, 2026

Methanol → HCID 18914100, compound

https://huagongshe.com/reaction/1292049

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantDichloromethaneHCID 6344—
ReactantHCID 18914101HCID 18914101—
ProductHCID 18914100HCID 18914100—

Reaction Steps

3-Chloromethyl-2-methyl-4-trifluoromethyl -pyridine from step 2 above was oxidized using the procedure as given in step 3 of Example 3. 3-Chloromethyl-2-methyl-4-trifluoromethyl-pyridine-N-oxide was obtained as a white solid (TLC Rf = 0.21 (97:3 CH2Cl2 :MeOH)).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05756497
Source datasetuspto-grants-1998_05
ORD IDord-1fc1d4c7d11b46728cbbb6ee17e530fe
Source noteuspto-grants-1998_05