HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → 5-Chloro 5,6,7,8-tetrahydroquinoline-N-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 5-Chloro-5,6,7,8-tetrahydroquinoline | HCID 18914103 | — |
| Product | 5-Chloro 5,6,7,8-tetrahydroquinoline-N-oxide | HCID 18914098 | — |
Reaction Steps
5-Chloro-5,6,7,8-tetrahydroquinoline from step 2 above was oxidized using the procedure as given in step 3 of Example 3. 5-Chloro 5,6,7,8-tetrahydroquinoline-N-oxide was obtained as a white solid (TLC Rf = 0.24 (97:3 CH2Cl2 : MeOH)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756497 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-a22b762ce17443f3b6d15f2552057df2 |
| Source note | uspto-grants-1998_05 |