HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 86752613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 86752614 | HCID 86752614 | — |
| Product | HCID 86752613 | HCID 86752613 | 97% |
Reaction Steps
A mixture of (IV) [7.06 g, 30.5 mmol] and excess 85% hydrazine hydrate in ethanol (300 mL) was heated under reflux (a precipitate formed). After cooling, the solid was collected by filtration and dried to give 4-methoxymethylpyridazino[4,5-b]indolizin-1-one (V, 6.81 g, 97%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756501 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-40c3c24f36b54f25852ede00bce0c489 |
| Source note | uspto-grants-1998_05 |