HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18914238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 9888723 | HCID 9888723 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 18914238 | HCID 18914238 | — |
Reaction Steps
1-[4-(4-fluorobenzyloxy)-3-isobutylbenzoyl]-4-isobutylpiperazine (3.18 g) was dissolved in diethyl ether (20 ml) and then 15 ml of 1N hydrogen chloride in ether was added. After this mixture was stirred for 10 minutes at room temperature, the resulting crystals were collected by filtration, thereby yielding 4.40 g of the aimed compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756505 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-140103b651f643aba8c624c890de300c |
| Source note | uspto-grants-1998_05 |