HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 18914285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-Benzyl-3-methyl-4-piperidone | HCID 560965 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18914285 | HCID 18914285 | — |
Reaction Steps
A mixture of 10 g of 1-benzyl-3-methyl-4-oxopiperidine and 8 mL of methyl iodide in 100 mL of acetone was stirred at 25° to 30° C. for 6 days then concentrated under reduced pressure to dryness. Drying under vacuum overnight gave 17 g of 1-methyl-1-benzyl-3-methyl-4-oxopiperidinium iodide as a beige foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756508 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-7007cdf93b7e44f98fcd70ef6fae3d39 |
| Source note | uspto-grants-1998_05 |