Potassium Carbonate → HCID 18354626, compound

HRID 1292130Notes

Reaction equation

HRID 1292130 reaction equation
[OH:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([NH2:7])=[O:6].C(=O)([O-])[O-].[K+].[K+].[N+:17]([C:20]1[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=1[CH2:22]Br)([O-:19])=[O:18]>C(#N)C>[N+:17]([C:20]1[CH:27]=[CH:26][CH:25]=[CH:24][C:21]=1[CH2:22][O:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([NH2:7])=[O:6])([O-:19])=[O:18]

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 77569alpha-Bromo-2-nitrotolueneHCID 3424033-Hydroxybenzamide

Product 1

HCID 18354626HCID 18354626, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

To 3-hydroxybenzamide (0.137 g; 1 mmol) was added potassium carbonate (0.138 g; 1 mmol) and 2-nitrobenzyl bromide (0.216 g; 1 mmol) in anhydrous acetonitrile (10 ml). The mixture was heated under reflux for 5 hours.

Workup

  1. temperatureThe mixture was heated
  2. temperatureunder reflux for 5 hours

Sources & evidence

ORD record
ord-cf18ff9bd4ae4a698a9746ec0a849ca1
Source dataset
uspto-grants-1998_05
Patent number
US05756510

Reaction notes

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