Aluminium lithium hydride → HCID 22857198, compound

Participants

Reaction Steps

Lithium aluminum hydride (5 equivalents) was allowed to react with a THF solution (20 ml) of trans-4,6,6a,8,9,10a-hexahydro-10a-methyl-1-(2,4,6-triisopropylphenylsulfonyl)-7H-indolo[3,4-gh][1.4]benzoxazin-8-one (1.2 g, 2.36 mmol). The residue thus obtained was subjected to a silica gel column chromatography, eluting with ethyl acetate, to afford 100 mg (15%) of the title compound.

Provenance & Evidence