HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonic acid monohydrate → HCID 18637511, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonic acid monohydrate | HCID 521998 | — |
| Reactant | HCID 6992292 | HCID 6992292 | — |
| Reactant | HCID 178464491 | HCID 178464491 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18637511 | HCID 18637511 | — |
Reaction Steps
A stirred suspension of carbobenzyloxyisoglutamine (28 g, 100 mmol) and p-toluenesulfonic acid monohydrate (1.9 g, 10 mmol) in 560 mL of absolute ethanol was gently refluxed for 12-14 hours or until TLC (1:5:94 HOAc/H2 /CH3CN) indicated that the reaction was complete.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756685 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-6ae4be46fb18430da72c2488a0f399ec |
| Source note | uspto-grants-1998_05 |