Aluminium lithium hydride → HCID 22857203, compound

Participants

Reaction Steps

Trans-7-ethyl-4,6,6a,8,9,10a-hexahydro-1-methoxy-10a-phenyl-7H-indolo[3,4-gh][1.4]benzoxazin-8-one (664 mg, 1.83 mmol) was reduced with LAH. The residue thus obtained was subjected to a silica gel column chromatography, eluting with n-hexane-ethyl acetate (3:1), to afford 74 mg (12%) of the title compound as a crude crystalline product (m.p.194-196 dec.)

Provenance & Evidence