HuagongsheHuagongshe Chemistry Print Report · For research reference only
Borane → HCID 21254087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Borane | HCID 6331 | — |
| Reactant | HCID 21254044 | HCID 21254044 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21254087 | HCID 21254087 | — |
Reaction Steps
To a stirred solution of N-benzyl-2-[2-(3,5-dimethylphenyl)-5-nitro-1H-indol-3-yl]-N-[4-(4-methanesulfonylaminophenyl)butyl]-2-oxo-acetamide (73 mg in 4 mL dry tetrahydrofuran) was added 1 mL of a 1M solution of borane in tetrahydrofuran and the mixture heated slowly to reflux on an oil bath.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756507 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-b940e6691cbf43e5b8d4b3b502013abc |
| Source note | uspto-grants-1998_05 |