HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 15170859, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 18915204 | HCID 18915204 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15170859 | HCID 15170859 | 91.1% |
Reaction Steps
To Compound c (7.84 g, 20.1 mmol) were added 100 ml of dioxane and 100 ml of 2N aqueous solution of sodium hydroxide, followed by heating under reflux for 10 minutes. After cooling, the mixture was neutralized, and deposited crystals were collected by filtration and recrystallized from dioxane-water to give 6.83 g (yield: 91%) of Compound 5 as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05756735 |
| Source dataset | uspto-grants-1998_05 |
| ORD ID | ord-551917864d4148229ee2bb385a31e9a6 |
| Source note | uspto-grants-1998_05 |