Phosphoric Acid → HCID 22445954, compound

HRID 1292592Notes

Reaction equation

HRID 1292592 reaction equation
[CH3:1][C:2]([CH3:11])([CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])[CH:3]([OH:5])[CH3:4].P(=O)(O)(O)O>C(OC(=O)CC)(=O)CC>[C:3]([O:5][CH:3]([C:2]([CH3:1])([CH3:11])[CH2:6][CH:7]=[C:8]([CH3:10])[CH3:9])[CH3:4])(=[O:5])[CH2:2][CH3:1]

Participants

4

Reactant 2

HCID 1004Phosphoric AcidHCID 18915869HCID 18915869, compound

Product 1

HCID 22445954HCID 22445954, compound

Reagents, catalysts & solvents 1

HCID 31263Propionic anhydrideSolvent

Procedure

From 46.8 g of 3,3,6-trimethyl-hept-5-en-2-ol, 70 ml of propionic anhydride and 0.1 ml of phosphoric acid analogously to Example 7.

Sources & evidence

ORD record
ord-07a85cc223784af79a99a426f8e7e98b
Source dataset
uspto-grants-1998_05
Patent number
US05756821

Reaction notes

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