HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2,4-Difluoro-phenoxy)-2-nitro-benzamide → HCID 58905135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2,4-Difluoro-phenoxy)-2-nitro-benzamide | HCID 58905142 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 58905135 | HCID 58905135 | 96.7% |
Reaction Steps
To compound (1C) (27 g, 0.09 mol) in EtOH was added palladium on activated carbon (2.7 g), and the mixture was stirred under hydrogen for 18 h. The suspension was filtered through celite and the filtrate concentrated and dried in vacuo to yield 23 g of 2-amino-5-(2,4-difluoro-phenoxy)-benzamide (1D).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238698B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-c7ee8ee6522443669ec5473ec4ef5dfb |
| Source note | uspto-grants-2007_07 |