Hydrochloric Acid → HCID 86584670, compound

HRID 1293045Notes

Reaction equation

HRID 1293045 reaction equation
[ClH:1].[CH:2]1([N:7]([CH:18]2[CH2:22][CH2:21][CH2:20][CH2:19]2)[CH2:8][CH2:9][NH:10]C(=O)OC(C)(C)C)[CH2:6][CH2:5][CH2:4][CH2:3]1>ClCCl>[ClH:1].[CH:2]1([N:7]([CH:18]2[CH2:22][CH2:21][CH2:20][CH2:19]2)[CH2:8][CH2:9][NH2:10])[CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22346208HCID 22346208, compound

Product 1

HCID 86584670HCID 86584670, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

Hydrogen chloride gas was passed through a stirred ice cold solution of tert-butyl 2-(dicyclopentylamino)ethylcarbamate (0.22 g, 0.74 mmol) (Preparation 52) in dichloromethane (15 ml) until the solution was saturated. The reaction mixture was allowed to warm to room temperature and then stirred for 1 hour. The solvent was removed under reduced pressure to give the title compound (0.15 g) as a brown foam.

Workup

  1. customThe solvent was removed under reduced pressure

Sources & evidence

ORD record
ord-2e5f6ffcee864674a8602edffadfa0c9
Source dataset
uspto-grants-2007_07
Patent number
US07238676B2

Reaction notes

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