Water → HCID 17838733, compound

Participants

Reaction Steps

To a solution of 3-benzylthio-1-dimethylcarbamoyl-1H-1,2,4-triazole (Example 1) (134 mg) in methylene chloride was added m-chloroperbenzoic acid (185 mg) with cooling it on ice, and the resulting mixture was stirred at room temperature for 4 hours. Ethyl acetate and water were added to the reaction mixture, which in turn was extracted with ethyl acetate. The organic layer was dried over sodium sulfate, and purified by a column chromatography (ethyl acetate/hexane=1/2) to yield the titled compound (69 mg) as a clear oil.

Provenance & Evidence