Methanol → HCID 178425949, compound

Participants

Reaction Steps

To a mixture of OXONE monopersulfate compound (3.02 g) and water (30 ml) was added dropwise a mixture of 3-(2,4,6-trimethylphenyl)thio-1H-1,2,4-triazole (Example 32-a) (1.08 g) and methanol (30 ml) with stirring it at room temperature. After the addition was completed, the reaction mixture was stirred for 3 hours, and water (20 ml) was added. Precipitated crystals were collected by filtration, and washed with water, ethyl acetate, and hexane in this order to yield the title compound (820 mg).

Provenance & Evidence