HCID 20134167, compound → HCID 57572314, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 3 of Example 1 from 5-fluoro-2-(4-fluorophenoxy)nicotinic acid (step 3 of Example 1) and methyl 4-(1-aminopropyl)benzoate: 1H-NMR (CDCl3) δ 8.33–8.26 (2H, m), 8.05–7.99 (3H, m), 7.39 (2H, d, J=8.4 Hz), 7.20–7.15 (4H, m), 5.15 (1H, q, J=7.3 Hz), 3.90 (3H, s), 1.92 (2H, dq, J=7.3, 7.3 Hz), 0.95 (3H, t, J=7.3 Hz); MS (ESI) m/z 427 (M+H)+, 425 (M−H)−.

Provenance & Evidence