HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenol → HCID 57572305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenol | HCID 9732 | — |
| Reactant | Methyl 5-bromo-2-chloronicotinate | HCID 2763343 | — |
| Product | HCID 57572305 | HCID 57572305 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 56 from methyl 5-bromo-2-chloronicotinate (J. Org. Chem. 1989, 54, 3618–3624) and 4-fluorophenol: 1H-NMR (CDCl3) δ 8.37 (1H, d, J=2.5 Hz), 8.27 (1H, d, J=2.5 Hz), 7.10 (2H, d, J=6.2 Hz), 3.95 (3H, s); MS (ESI) m/z 326 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238714B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-0bce2addbd76456d93d90e8da96075b6 |
| Source note | uspto-grants-2007_07 |