HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 2,5-Dichloronicotinate → Methyl 5-chloro-2-(3-chlorobenzyl)nicotinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 2,5-Dichloronicotinate | HCID 2764318 | — |
| Reactant | HCID 178478087 | HCID 178478087 | — |
| Product | Methyl 5-chloro-2-(3-chlorobenzyl)nicotinate | HCID 57572306 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 2 of Example 58 from methyl 2,5-dichloronicotinate and 3-chlorobenzylzinc chloride: 1H-NMR (CDCl3) δ 8.65 (1H, d, J=2.6 Hz), 8.17 (1H, d, J=2.6 Hz), 7.26–7.12 (4H, m), 4.52 (2H, s), 3.89 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238714B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-ca5931eefde24aaaab44fc0110a31838 |
| Source note | uspto-grants-2007_07 |