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HRID1293224

反应详情

EQUATION

反应方程式

HRID 1293224 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1cc(Cl)ccc1Oc1cccc(Cl)c1
HCID12602965

未命名化合物

结构：COC(=O)c1ccc([C@H](C)N)cc1.Cl
HCID57462942

Methyl 4-[(1S)-1-aminoethyl]benzoate--hydrogen chloride (1/1)

C10H14ClNO2

PRODUCTS

生成物

1
结构：COC(=O)c1ccc([C@H](C)NC(=O)c2cc(Cl)ccc2Oc2cccc(Cl)c2)cc1
HCID57572255

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in step 3 of Example 1 from 5-chloro-2-(3-chlorophenoxy)benzoic acid (step 2) and methyl 4-[(1S)-1-aminoethyl]benzoate hydrochloride (step 3 of Example 5): 1H-NMR (CDCl3) δ 8.17 (1H, d, J=2.8 Hz), 7.93 (2H, m), 7.65 (1H, d, J=7.4 Hz), 7.42–7.19 (5H, m), 6.97–6.81 (3H, m), 5.32 (1H, dq, J=7.4, 6.9 Hz), 3.90 (3H, s), 1.49 (3H, d, J=6.9 Hz).