2,5-Dichlorophenol → HCID 69415791, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 2,5-dichlorophenol: 1H-NMR (CDCl3) δ 8.55 (1H, d, J=2.8 Hz), 8.34 (1H, d, J=2.6 Hz), 8.27–7.99 (3H, m), 7.46–7.43 (3H, m), 7.35 (1H, d, J=2.3 Hz), 7.29–7.25 (1H, m), 5.44–5.34 (1H, m), 3.90 (3H, s), 1.61 (3H, d, J=6.9 Hz).

Provenance & Evidence