3,4-Dichlorophenol → HCID 69415999, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 3,4-dichlorophenol: 1H-NMR (CDCl3) δ 8.52 (1H, d, J=2.6 Hz), 8.13 (1H, d, J=2.8 Hz), 8.00 (2H, dd, J=6.7, 1.9 Hz), 7.93 (1H, d, J=7.4 Hz), 7.51 (1H, d, J=8.7 Hz), 7.42 (2H, d, J=8.1 Hz), 7.30 (1H, d, J=2.6 Hz), 7.03 (1H, dd, J=8.7, 2.6 Hz), 5.42–5.31 (1H, m), 3.90 (3H, s), 1.60 (3H, d, J=6.9 Hz).

Provenance & Evidence