3,5-Dichlorophenol → HCID 69415878, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 2 of Example 45 from methyl 4-((1S)-1-{[(2,5-dichloropyridin-3-yl)carbonyl]amino}ethyl)benzoate (step 1 of Example 48) and 3,5-dichlorophenol: 1H-NMR (CDCl3) δ 8.54 (1H, d, J=2.6 Hz), 8.16 (1H, d, J=2.8 Hz), 8.02 (2H, dd, J=6.6, 1.8 Hz), 7.84 (1H, d, J=7.3 Hz), 7.42 (2H, d, J=8.6 Hz), 7.31 (1H, t, J=1.8 Hz), 7.08 (2H, d, J=1.8 Hz), 5.41–5.31 (1H, m), 3.91 (3H, s), 1.60 (3H, d, J=6.9 Hz).

Provenance & Evidence