HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Difluorophenol → Methyl 5-chloro-2-(3,4-difluorophenoxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Difluorophenol | HCID 75927 | — |
| Reactant | Methyl 5-chloro-2-fluorobenzoate | HCID 21525433 | — |
| Product | Methyl 5-chloro-2-(3,4-difluorophenoxy)benzoate | HCID 69415844 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 67 from methyl 5-chloro-2-fluorobenzoate and 3,4-difluorophenol: 1H-NMR (CDCl3) δ 7.92 (1H, d, J=2.8 Hz), 7.46 (1H, dd, J=8.7, 2.8 Hz), 7.11 (1H, q, J=9.1 Hz), 6.95 (1H, d, J=8.7 Hz), 6.85–6.72 (1H, m), 6.71–6.59 (1H, m), 3.83 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238714B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-d4a619b8d94540dd95600e9a2be95da1 |
| Source note | uspto-grants-2007_07 |