HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Difluorophenol → HCID 69417845, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Difluorophenol | HCID 94392 | — |
| Reactant | Methyl 2-Fluoro-5-nitrobenzoate | HCID 11217860 | — |
| Product | HCID 69417845 | HCID 69417845 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 67 from methyl 2-fluoro-5-nitrobenzoate (J. Org. Chem. 1990, 55, 2034.) and 2,6-difluorophenol: 1H-NMR (CDCl3) δ 8.83 (1H, d, J=2.8 Hz), 8.25 (1H, dd, J=9.2, 2.8 Hz), 7.32–7.20 (1H, m), 7.12–7.02 (2H, m), 6.82 (1H, d, J=9.2 Hz), 3.98 (3H, s); MS (ESI) m/z 310 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238714B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a2e622db82bf462790cbdc09507dced6 |
| Source note | uspto-grants-2007_07 |