HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 69282843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 69280150 | HCID 69280150 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69282843 | HCID 69282843 | 85.6% |
Reaction Steps
To a solution of methyl-9-benzyl-1-ethoxy-9H-4-carbazolecarboxylate (728 mg, 2.027 mmoles), in methanol (10 ml), aqueous sodium hydroxide (81 mg, 2.027 mmoles) was added and the reaction mixture was refluxed for 1 hr. Methanol was evaporated under reduced pressure, the reaction mixture was acidified with 1N HCl and filtered to yield 599 mg of title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238725B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-69d8a4714d2341749ce12a82aa4c5639 |
| Source note | uspto-grants-2007_07 |