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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1293482Generated: October 30, 2026

Sodium Hydroxide → HCID 69282843, compound

https://huagongshe.com/reaction/1293482

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium HydroxideHCID 14798—
ReactantHCID 69280150HCID 69280150—
SolventMethanolHCID 887—
ProductHCID 69282843HCID 6928284385.6%

Reaction Steps

To a solution of methyl-9-benzyl-1-ethoxy-9H-4-carbazolecarboxylate (728 mg, 2.027 mmoles), in methanol (10 ml), aqueous sodium hydroxide (81 mg, 2.027 mmoles) was added and the reaction mixture was refluxed for 1 hr. Methanol was evaporated under reduced pressure, the reaction mixture was acidified with 1N HCl and filtered to yield 599 mg of title compound as an off-white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07238725B2
Source datasetuspto-grants-2007_07
ORD IDord-69d8a4714d2341749ce12a82aa4c5639
Source noteuspto-grants-2007_07