HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 57091572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 57192749 | HCID 57192749 | — |
| Product | HCID 57091572 | HCID 57091572 | — |
Reaction Steps
4 g of 4-(3-chloropropylthio)resorcin and 8 ml of morpholine are heated for two hours at 100° C. The mixture is poured into ice-cold water and extracted with ethyl acetate. The organic phases are washed, dried and concentrated under vacuum. The yellow oil is crystallized from ethyl acetate to lead to white crystals having a melting point of: 99° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468472 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-747efc1a7da74df8bde2a7878082bcbd |
| Source note | uspto-grants-1995_11 |