HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 17755864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Chloro-5-nitropyridine | HCID 78308 | — |
| Reactant | 4-Amino-3-Nitrophenol | HCID 3758882 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 17755864 | HCID 17755864 | — |
Reaction Steps
2-Nitro-4-hydroxyaniline was reacted with 2-chloro-5-nitropyridine and K2CO3 in DMF at rt, followed by hydrogenation over Pd/C in MeOH, afforded the title compound; MS m/e 217 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238813B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-36746e833c704596986dcc9ee71cbe81 |
| Source note | uspto-grants-2007_07 |