HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25128463, compound → HCID 17861339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25128463 | HCID 25128463 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 17861339 | HCID 17861339 | 84% |
Reaction Steps
A mixture of ethyl (E)-3-(2-benzyloxy-4-methoxymethoxyphenyl)-2-propenoate (14.80 g), 5% palladium carbon (20.0 g) and ethanol (300 mL) was subjected to catalytic hydrogenation at room temperature and 1 atm. After filtering off the catalyst, the solvent was evaporated under reduced pressure to give ethyl 3-(2-hydroxy-4-methoxymethoxyphenyl)propionate as a colorless oil (9.17 g, 84%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07238716B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-93907ef5e8f54ae0b349d67533477dc3 |
| Source note | uspto-grants-2007_07 |