HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 13007955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | 1-[3-(pyrrolidin-1-yl)propyl]-1,4-diazepane | HCID 2737251 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13007955 | HCID 13007955 | 95.5% |
Reaction Steps
Fluoronitrobenzene (5.56 g, 39.43 mmol) is dissolved in water, and then potassium carbonate (6.55 g, 47.31 mmol) and 1-(3-pyrrolidinopropyl)-homopiperazine (10 g, 47.31 mmol) are added. The medium is heated at 85° for 4 hours and then cooled to room temperature. The medium is filtered and a yellow solid is recovered after drying in a vacuum oven at 45° C. (12.5 g, yield=95.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241317B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-c9a8c03537d246feb7c071f9bc17f2e0 |
| Source note | uspto-grants-2007_07 |