HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1294402Generated: November 2, 2026
Potassium Carbonate → HCID 13007959, compound
https://huagongshe.com/reaction/1294402
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | 2-(1,4-Diazepan-1-yl)ethan-1-ol | HCID 2736550 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13007959 | HCID 13007959 | 91.7% |
Reaction Steps
Fluoronitrobenzene (2.03 g, 14.4 mmol) is dissolved in water (10 ml), and then potassium carbonate (2.4 g, 17.3 mmol) and 1-(2-hydroxyethyl)-homopiperazine are added. The medium is heated at 95° C. for 4 hours and then cooled to room temperature and filtered. A dark orange-coloured powder is recovered which is placed in the oven (3.5 g, yield=91.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07241317B2 |
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| Source dataset | uspto-grants-2007_07 |
|---|
| ORD ID | ord-42aa3a42d33a4141a14469808b5fe89d |
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| Source note | uspto-grants-2007_07 |
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