Dimethylamine, hydrochloride → HCID 66879286, compound
Reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:22])[N:13]([C:15]3[CH:16]=[N:17][CH:18]=[C:19](F)[CH:20]=3)[CH:14]=2)[CH:5]=[CH:6][CH:7]=1.Cl.[CH3:24][NH:25][CH3:26]>>[Cl:1][C:2]1[CH:3]=[C:4]([C:8]#[C:9][C:10]2[N:11]=[C:12]([CH3:22])[N:13]([C:15]3[CH:20]=[C:19]([N:25]([CH3:26])[CH3:24])[CH:18]=[N:17][CH:16]=3)[CH:14]=2)[CH:5]=[CH:6][CH:7]=1Participants
3
Procedure
The title compound, MS: m/e=337.3 (M+), was prepared in accordance with the general method of example 27 from 3-[4-(3-chloro-phenylethynyl)-2-methyl-imidazol-1-yl]-5-fluoro-pyridine and dimethylamine hydrochloride.
Sources & evidence
- ORD record
- ord-09e0210ed1b04d819e34cafa2e72bd79
- Source dataset
- uspto-grants-2007_07
- Patent number
- US07241760B2
Reaction notes
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