HRID1294565

反应详情

EQUATION

反应方程式

HRID 1294565 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1.44 g (10.2 mmol) (2-amino-6-fluoro-phenyl)-methanol are dissolved in 120 ml chloroform, combined with 4.43 g (51 mmol) manganese(IV)-oxide and stirred for 2 days at ambient temperature. Then excess manganese(IV)-oxide is filtered off through Celite and the solvent is eliminated in vacuo.

WORKUP

后处理

  1. filtrationThen excess manganese(IV)-oxide is filtered off through Celite