HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Amino-6-fluorophenyl)methanol → 2-Amino-6-fluorobenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Amino-6-fluorophenyl)methanol | HCID 11521092 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | 2-Amino-6-fluorobenzaldehyde | HCID 21719475 | — |
Reaction Steps
1.44 g (10.2 mmol) (2-amino-6-fluoro-phenyl)-methanol are dissolved in 120 ml chloroform, combined with 4.43 g (51 mmol) manganese(IV)-oxide and stirred for 2 days at ambient temperature. Then excess manganese(IV)-oxide is filtered off through Celite and the solvent is eliminated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241769B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-b108d51035b343a5afea5c1bd1d77e49 |
| Source note | uspto-grants-2007_07 |