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HRID1294804

反应详情

EQUATION

反应方程式

HRID 1294804 的结构方程式

REACTANTS

反应物

3
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：Cl.c1ccc2c(N3CCNCC3)nsc2c1
HCID11521711

3-(1-Piperazinyl)-1,2-benzisothiazole monohydrochloride

C11H14ClN3S

结构：CCN(CC)c1ccc(S(C)(=O)=O)cc1C(=O)O
HCID57445276

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)c1ccc(S(C)(=O)=O)cc1C(=O)N1CCN(c2nsc3ccccc23)CC1
HCID58906301

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

Prepared in analogy to example 1.1 b) from 2-diethylamino-5-methanesulfonyl-benzoic acid (Example 2.5) and 3-piperazin-1-yl-benzo[d]isothiazole hydrochloride (CA=87691-88-1) in acetonitrile. Chromatography (SiO2; ethyl acetate) yields the title compound as a colorless solid. MS (m/e): 473.4 (M+H+; 100%)