HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,3-difluoro-N-methoxy-N-methylbenzamide → (2,3-Difluorophenyl)-(4-methoxy-3-methyl-phenyl)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,3-difluoro-N-methoxy-N-methylbenzamide | HCID 62661190 | — |
| Reactant | HCID 178491913 | HCID 178491913 | — |
| Product | (2,3-Difluorophenyl)-(4-methoxy-3-methyl-phenyl)-methanone | HCID 55101193 | — |
Reaction Steps
Prepared according to Method A step B from 2,3-difluoro-N-methoxy-N-methyl-benzamide (2.5 g, 12.4 mmol) and 4-methoxy-3-methyl-phenylmagnesium bromide (26 mL, 0.5 M in THF) to give 0.97 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-f6a2a6fa2e0945028d75ed3c7ba7ef5b |
| Source note | uspto-grants-2007_07 |