HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-fluoro-N-methoxy-N,3-dimethylbenzamide → (2-Fluoro-3-methylphenyl)(4-methoxy-2-methylphenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-fluoro-N-methoxy-N,3-dimethylbenzamide | HCID 80718058 | — |
| Reactant | HCID 178491917 | HCID 178491917 | — |
| Product | (2-Fluoro-3-methylphenyl)(4-methoxy-2-methylphenyl)methanone | HCID 68883841 | — |
Reaction Steps
Prepared according to Method A step B from 2- fluoro-3-methyl-N-methoxy-N-methyl-benzamide (3.10 g, 15.7 mmol) and 4-methoxy-2-methyl-phenylmagnesium bromide (40 mL, 0.5 M in THF) to give 1.17 g of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-a6798f13e8e949408f279fe6dfaab93a |
| Source note | uspto-grants-2007_07 |