HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-bromo-2-fluoro-N-methoxy-N-methylbenzamide → (3-Bromo-2-fluorophenyl)(4-methoxy-2-methylphenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-bromo-2-fluoro-N-methoxy-N-methylbenzamide | HCID 57825253 | — |
| Reactant | HCID 178491917 | HCID 178491917 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | (3-Bromo-2-fluorophenyl)(4-methoxy-2-methylphenyl)methanone | HCID 68883872 | — |
Reaction Steps
Prepared according to Method A step B from 3-bromo-2-fluoro-N-methoxy-N-methylbenzamide (8 g, 31 mmol) and 2-methyl-4-methoxyphenyl magnesium bromide ((70 ml, 0.5 M in THF) to give 3.58 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07241791B2 |
| Source dataset | uspto-grants-2007_07 |
| ORD ID | ord-97321b99fd034ecaae22f29428ec289e |
| Source note | uspto-grants-2007_07 |