2-Hydrazinoethanol → HCID 136358435, compound

HRID 1294878Notes

Reaction equation

HRID 1294878 reaction equation
O[C:2]1[CH:17]=[C:16]([OH:18])[CH:15]=[CH:14][C:3]=1[C:4]([C:6]1[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][C:7]=1[OH:13])=O.C([O-])(=O)C.[Na+].[OH:24][CH2:25][CH2:26][NH:27][NH2:28]>>[OH:18][C:16]1[CH:17]=[C:2]2[C:3]([C:4]([C:6]3[CH:11]=[CH:10][C:9]([OH:12])=[CH:8][C:7]=3[OH:13])=[N:28][N:27]2[CH2:26][CH2:25][OH:24])=[CH:14][CH:15]=1

Participants

4

Reactant 3

HCID 80172-HydrazinoethanolHCID 85712,2',4,4'-TetrahydroxybenzophenoneHCID 517045Sodium Acetate

Product 1

HCID 136358435HCID 136358435, compoundYield 14%

Procedure

Prepared according to Method B from 2,2′,4,4′-tetrahydroxybenzophenone (0.123 g, 0.5 mmol), sodium acetate (0.164 g, 2 mmol) and 2-hydroxyethylhydrazine (0.085 g, 1.0 mmol) to give 0.020 g of product as a white solid

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-de8631e0ba3a4f93a200c4536ff20a07
Source dataset
uspto-grants-2007_07
Patent number
US07241791B2

Reaction notes

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